邻菲啰啉在测定亚铁中的保护效果          下载免费PDF全文

张会堂  刘瑄  刘渝燕  刘晶  巩宝珍 《山东国土资源》2003,19(1):54-56

样品在分解过程中 ,亚铁易被空气部分氧化 ,致使测试结果偏低 ,采用在HF H2 SO4溶矿过程中加入邻菲卟罗啉 ,与亚铁形成络合物 ,对保护亚铁具有较好的效果。拟定了在塑料坩埚中加邻菲卟罗啉、H2 SO4及HF ,中高温电热板溶矿 ,容量法测定样品中的亚铁 ,方法精密度为 0 .2 3% ,样品加标准回收率 98.8%～ 10 1.9%。此方法具有较好的应用效果  相似文献   

Prediction Test for the Two Extremely Strong Solar Storms in October 2003   总被引：2，自引：0，他引：2  

Yanqiong Xie  Fengsi Wei  Xueshang Feng  Dingkun Zhong 《Solar physics》2006,234(2):363-377

In late October and early November 2003, a series of space weather hazard events erupted in solar-terrestrial space. Aiming at two intense storm (shock) events on 28 and 29 October, this paper presents a Two-Step method, which combines synoptic analysis of space weather–`observing’ and quantitative prediction – ‘palpating’, and uses it to test predictions. In the first step, ‘observing’, on the basis of observations of the source surface magnetic field, interplanetary scintillation (IPS) and ACE spacecraft, we find that the propagation of the shock waves is asymmetric and northward relative to the normal direction of their solar sources due to the large-scale configuration of the coronal magnetic fields, and the Earth is located near the direction of the fastest speed and greatest energy of the shocks. Being two fast ejection shock events, the fast explosion of extremely high temperature and strong magnetic field, and background solar wind velocity as high as 600 and 1000 km s⁻¹, are also helpful to their rapid propagation. According to the synoptic analysis, the shock travel times can be estimated as 21 and 20 h, which are close to the observational results of 19.97 and 19.63 h, respectively. In the second step, ‘palpating’, we adopt a new membership function of the fast shock events for the ISF method. The predicted results here show that for the onset time of the geomagnetic disturbance, the relative errors between the observational and the predicted results are 1.8 and 6.7%, which are consistent with the estimated results of the first step; and for the magnetic disturbance magnitude, the relative errors between the observational and the predicted results are 4.1 and 3.1%, respectively. Furthermore, the comparison among the predicted results of our Two-Step method with those of five other prevailing methods shows that the Two-Step method is advantageous in predicting such strong shock event. It can predict not only shock arrival time, but also the magnitude of magnetic disturbance. The results of the present paper tell us that understanding the physical features of shock propagation thoroughly is of great importance in improving the prediction efficiency.  相似文献   

有关边界层问题中一类奇异积分方程新的存在性结果     

石丽莉  张高勋 《成都信息工程学院学报》2006,21(6):891-896

对边界层理论新结果中出现的一类奇异积分方程w（t）=∫1 t（1-s）（λ＋λs＋s）/w（s）ds＋（1-t）∫t 0s/w（s）ds,t∈（0,1）进行讨论，并得出了上述方程在λ∈（-1/2,0）上正解存在性的新结果。  相似文献   

Petroleum exploration potential of Tamtsag Basin     

SUN Guo-qing  GUO Qing-xia  ZHANG Ya-jin  ZHAO Hong-wen 《世界地质(英文版)》2004,7(1)

The Tamtsag Basin is located in the extreme eastern portion of the Mongolia. The Basin and its counterpart in China (the Hailar Basin) are united a whole basin on the structural setting. In recent years, the Tamtsag Basin attracts more and more attention with the important exploration discovered in the 19th block by SOCO and in Hailar Basin of China. This paper discusses the exploration potential of Tamtsag Basin from the viewpoint of petroleum geology.  相似文献   

星风吸积引起的钡星重元素超丰     

常瑞香  张波  彭秋和 《中国天文和天体物理学报》1997,(3)

首先指出目前星风吸积模型中理论上的不自洽，考虑到δｒ≠０，重新推导轨道参量变化方程，消去了理论上的不自洽．提出一个新模型：首次将星风吸积同内禀ＡＧＢ星核合成模型结合起来计算钡（Ｂａ）星的重元素超丰，并将计算结果与观测值进行了比较．各参量按标准情况取值时，计算结果不太理想．取Ｂｏｎｄｉｈｏｙｌｅ吸积率的０．５倍或取较大的星风速率时，对于较长轨道周期（Ｐ＞１０００天）的Ｂａ星，计算结果与观测值基本符合；而较短轨道周期（Ｐ＜６００天）的Ｂａ星，其重元素超丰机制可能是盘吸积  相似文献   

Isotopic evidence for holocene climatic changes in Bosten Lake, Southern Xinjiang, China     

Zhong Wei  Xiong Heigang 《中国地理科学(英文版)》1997,8(2):176-182

Based on the δ¹³C and δ¹⁸O fluctuation of lacustrine carbonate, CaCO₃ content and sporo-pollen data, a palaeoclimatic history of Bosten Lake during the Holocene has been outlined, several stages of climatic changes are divided, and the following result es are obtained: (1) Palaeoclimatic changes revealed by carbonate isotope around Bosten Lake are basically identical with that revealed by other geological records in Xinjiang. Environmental changes presented apparent Westlies Style model: during cold period, relative humidity increased, δ¹⁸O, δ¹³C and CaCO₃ appeared low; but in warm periods, the dry regime aggravated. (2) The temperature reflected by δ¹⁸O exist evident features being increase in the late period during the Holocene. Together with the δ¹³C, pollen and CaCO₃ analyses, several cold and warm phases which are of broad regional significance can be identified. The warm peaks occurred at about 11.0 ka B.P., 9.4 ka B.P., 7.5 ka B.P., 5.0 ka B.P., 3.0 ka B.P. and 2.0 ka B.P.; the cold peaks at 11.5 ka B.P., 10.5 ka B.P., 8.8 ka B.P., 5.5 ka B.P., 3.3 ka B.P., 2.2 ka B.P. and 1.5 ka B.P.. (3) Several climatic events with the nature of “abrupt climatic changes” are revealed in the periods of 11.0 ka B.P. −10.5 ka B.P., 9.4 ka B.P. −8.8 ka B.P., 5.5 ka B.P. −5.0 ka B.P. and 2.0 ka B.P. −1.5 ka B.P.. (4) The results show that carbonate isotopic record of lacustrine sediment in arid area is very sensitive to climatic changes, and may be play a very important role in understanding the features and mechanism of palaeoclimatic changes.  相似文献   

北部湾北部海上油田发现历程     

钟铿  潘其云 《南方国土资源》1997,(2)

北部湾北部海上油田的开发工作始于５０年代，６０～７０年代作了大量地质工作。改革开放后，油气勘查取得突破性进展。累计发现油气构造６个，含油面积超过４０ｋｍ２，石油地质储量约４亿ｔ，已开发油田２个，揭开我国南方油气资源开发序幕  相似文献   

加强基础科学研究,走向国际     

张祖勋 《地球信息科学学报》1997,(1):68-68

今天能够参加中国科学中心的第一次会议,同时在此之前跟着陈先生,廖院士、何秘书长一块去莫斯科参加这次欧亚科学院院士大会,被选为欧亚科学院院士,对我来说是很大的荣誉。这次到莫斯科参加大会,感受很深,刚才大家谈到俄罗斯,原苏联,它的整个科学,曾对我国的发展,有一段起过很大的影响。这次去后我的感受很深,俄罗斯人民对我们的友好感情非常深。  相似文献   

ANALYSIS OF DRIVING FORCES ON THE CHANGE OF HISTORICAL FARMLAND USE IN SHANDONG PROVINCE DURING THE QING DYNASTY (1644-1911)     

ZHANG Xue-in  GE Quan-heng  ZHENG Jing-un 《中国地理科学(英文版)》2003,13(3)

1INTRODUCTIONTheIGBP-IHDP(InternationalGeosphere-BiosphereProgramme,andInternationalHumanDimensionPro-gramme)jointproject—LUCC(landuse/coverchange)isaninterdisciplinaryprogramdesignedtoimprovetheunderstandingofthedynamicsofland-useandland-coverchangeasinputstoandconsequencesofglobalenvironmentalchangeandsustainabledevelopment(CHARLOTTE,2002).Inparticularthedifferentbio-geochemicalmodeling(e.g.theglobalcarboncycle)ac-tivitiesandcomparativestudies,suchasthoseconduct-edbyIGBP-G…  相似文献   

小行星(360)Carlova自转参数的测定     

王晓彬  张西亮 《天文学报》2006,47(2):202-211

小行星自转参数的资料不仅可以为小行星碰撞演化提供数据,还可以为太阳系的演化研究提供依据．利用云南天文台1米望远镜对主带碳类小行星(360)Carlova进行了新的CCD测光观测,结合前人的测光资料,利用Epoch-方法对(360)的自转参数进行了反演计算,得到该小行星自转的恒星周期为0．25780417±0．00000003天,自转轴的黄道坐标为(95°±3,°40°±1°)．新的结果与前人的结果相比较为一致,其精度稍高于以前的估算结果．  相似文献